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Reactive extraction of itaconic acid using tri-n-butyl phosphate and aliquat 336 in sunflower oil as a non-toxic diluent

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논문

Reactive extraction of itaconic acid using tri-n-butyl phosphate and aliquat 336 in sunflower oil as a non-toxic diluent

학술지

Journal of chemical technology and biotechnology

저자명

Wasewar, Kailas L.; Shende, Diwakar; Keshav, Amit

초록

<P><B>Abstract</B></P><P>Itaconic acid finds a place in various industrial applications. It can be produced by biocultivation in a clean and environment friendly route but recovery of the acid from the dilute stream of the bioreactor is an economic problem. Reactive extraction is a promising method to recover carboxylic acid but suffers from toxicity problems of the diluent and extractant employed. So there is need for a non&#8208;toxic extractant and diluent or a combination of less toxic extractants in a non&#8208;toxic diluent that can recover acid efficiently. Effect of different extractants: tri&#8208;<I>n</I>&#8208;butylphosphate (TBP) (an organophosporous compound) and Aliquat 336 (a quaternary amine) in sunflower oil was studied to find the best extractant&ndash;sunflower oil combination. Equilibrium complexation constant, <I>K</I><SUB>E</SUB>, values of 1.789 and 2.385 m<SUP>3</SUP> kmol<SUP>&minus;1</SUP>, respectively, were obtained for itaconic acid extraction using TBP and Aliquat 336 in sunflower oil. The problem of toxicity in reactive extraction can be reduced by using a natural non&#8208;toxic diluent (sunflower oil) with the extractant. Copyright &copy; 2010 Society of Chemical Industry</P>

발행연도

2011

발행기관

John Wiley Sons, Ltd.

ISSN

0268-2575

ISSN

1097-4660

86

2

페이지

pp.319-323

주제어

itaconic acid; reactive extraction; toxicity; sunflower oil; tri&#x2010; n&#x2010; butylphosphate; Aliquat 336;

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논문; 2010-08-25

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