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Evaluation of stability of (1R,2 S)-(-)-2-methylamino-1-phenyl-1-propanol hydrochloride in plasma and urine samples-inoculated with Escherichia coli using high-performance liquid chromatography (HPLC)

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논문

Evaluation of stability of (1R,2 S)-(-)-2-methylamino-1-phenyl-1-propanol hydrochloride in plasma and urine samples-inoculated with Escherichia coli using high-performance liquid chromatography (HPLC)

학술지

World journal of microbiology & biotechnology

저자명

Almaary, Khalid S.; Alharbi, Naiyf S.; Al-Huwaymil, Rayan M.; Kadaikunnan, Shine; Alobaidi, Ahmed S.; Khaled, Jamal M.

초록

<P><B>Abstract</B><P>The preservation of drug stability in biological evidence during the processes of collection and storage poses a substantial obstacle to the progress of forensic investigations. In conjunction with other constituents, the microorganisms present in the samples play a vital role in this investigation. The present investigation employed the high-performance liquid chromatography (HPLC) technique to assess the stability of (1R,2 S)-(-)-2-methylamino-1-phenyl-1-propanol hydrochloride in plasma and urine samples that were inoculated with <I>Escherichia coli</I>. These samples were subjected to storage conditions of 37 &deg;C for 48 h and &#x2212; 20 &deg;C for a duration of 6 months. Minimal inhibitory concentration (MIC) and Minimal bactericidal concentration (MBC) of MPPH against <I>E. coli</I> were determined using microdilution method. The stability of MPPH in plasma and urine samples inoculated with <I>E. coli</I> was investigated using HPLC method. The results showed the MIC and MBC of MPPH were 87.5 ± 25 ppm and 175 ± 50 ppm, respectively. While MPPH remained stable in plasma for 48 h at 37 &deg;C, it showed a notable decrease of about 11% in stability when stored in urine for the same period and temperature. From the beginning of the first month, a decrease in the stability of the compound appeared in all samples that were stored at &#x2212; 20 &deg;C, and the decrease reached 7% for plasma samples and about 11% for urine samples. The decrease in the stability reached its peak in the sixth month, reaching more than 30% and 70% of plasma and urine samples preserved at &#x2212; 20 &deg;C. This work concluded that <I>E. coli</I> can negatively affect the stability of MPPH in plasma and urine samples. This may lead to incorrect conclusions regarding the analysis of biological samples in criminal cases.</P></P>

발행연도

2024

발행기관

Springer-Verlag

ISSN

0959-3993

ISSN

1573-0972

40

3

페이지

pp.96

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1 2023-12-11

논문; 2024-02-13

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