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Merger of Whole Cell Biocatalysis with Organocatalysis Upgrades Alcohol Feedstocks in a Mild, Aqueous, One-Pot Process

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논문

Merger of Whole Cell Biocatalysis with Organocatalysis Upgrades Alcohol Feedstocks in a Mild, Aqueous, One-Pot Process

학술지

ACS sustainable chemistry et engineering

저자명

Stewart, Kelsey N.; Hicks, Emily G.; Domaille, Dylan W.

초록

<P>Biosynthetic methods have the potential to deliver value-added chemicals from renewable feedstocks. However, despite major advances in metabolic engineering and synthetic biology, the rapid engineering of microbes to deliver high yields and titers of target compounds remains as a challenge. Here, we disclose a new chemical catalysis-based strategy for expanding the types of products available from unmodified microorganisms. By combining <I>Gluconobacter oxidans</I> as a whole cell biocatalyst in a single pot with a lysine organocatalyst, we demonstrate that aqueous solutions of C<SUB>n</SUB> n-aliphatic alcohols are converted to C<SUB>2n</SUB> &alpha;,&beta;-unsaturated aldehydes in a single pot in mild conditions. This carbon-doubling reaction works with a range of C<SUB>2</SUB>-C<SUB>6</SUB> alcohol substrates. In the absence of the lysine organocatalyst, only n-aliphatic carboxylic acids are observed, indicating that the organocatalyst intercepts metabolic intermediates and redirects flux toward target chemicals. Taken together, our work reveals a new strategy of flux redirection to expand the scope of products from biosynthetic processes.</P><P>Biocompatible catalysts can intercept microbially produced metabolites and upgrade them to high-volume chemicals in mild, aqueous conditions.</P><BR>[FIG OMISSION]</BR>

발행연도

2020

발행기관

American Chemical Society

ISSN

2168-0485

8

10

페이지

pp.4114-4119

주제어

Biocatalysis; Gluconobacter oxidans; Organocatalysis; Upgrading; Biocompatible chemistry

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1 2023-12-11

논문; 2020-02-20

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