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Simultaneous Adsorption and Fixation of Aspergillus oryzae β-Galactosidase on Polyelectrolyte-Layered Polysulfone Hollow-Fiber Membrane

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논문

Simultaneous Adsorption and Fixation of Aspergillus oryzae β-Galactosidase on Polyelectrolyte-Layered Polysulfone Hollow-Fiber Membrane

학술지

Industrial & engineering chemistry research

저자명

Gonawan, Fadzil Noor; Kamaruddin, Azlina Harun; Abu Bakar, Mohamad Zailani; Abd Karim, Khairiah

초록

<P>A simple procedure involving simultaneous adsorption and fixation was developed to immobilize &beta;-galactosidase (&beta;-Gal) from <I>Aspergillus oryzae</I> on a polysulfone hollow-fiber membrane module for converting lactose to galacto-oligosaccharides. Polyethylenimine was used as a polyelectrolyte intermediate layer to provide a positively charged character for &beta;-Gal adsorption. &beta;-Gal adsorbed on polyethylenimine layer was then fixed with cross-linking by glutaraldehyde. The concentrations of polyethylenimine, glutaraldehyde, and &beta;-Gal were significant parameters to achieve high activity yield. The optimum concentration of polyethylenimine and glutaraldehyde were determined as 5% (w/v) and 15% (v/v), respectively. The activity yield on the membrane surface increases as the concentration of &beta;-Gal used during adsorption and fixation increased. The highest activity yield obtained was 1.26 IU cm<SUP>&ndash;2</SUP> at 5 mg mL<SUP>&ndash;1</SUP> of &beta;-Gal concentration. The activity yield is proportionally dependent on the concentration of the &beta;-Gal employed. Moreover, the immobilized &beta;-Gal exhibited higher specific productivity and stable transgalactosylation activity compared with free &beta;-Gal during the lactose-catalyzed conversion reaction.</P>

발행연도

2016

발행기관

American Chemical Society

ISSN

0888-5885

ISSN

1520-5045

55

1

페이지

pp.21-29

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1 2023-12-11
2 2023-12-11

논문; 2016-12-31

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