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Biotransformation of isoflavone using enzymatic reactions

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논문

Biotransformation of isoflavone using enzymatic reactions

학술지

Molecules a journal of synthetic chemistry and natural product chemistry

저자명

Roh, Changhyun

초록

<P>The roles of cytochrome P450 monooxygenases (CYPs) from <I>Streptomyces</I> spp. which are called the “treasure islands” for natural products for medicine and antibiotics are not well understood. Substrate specificity studies on CYPs may give a solution for elucidation of their roles. Based on homology sequence information, the CYP105D7 of a soluble cytochrome P450 known as heme protein from <I>Streptomyces avermitilis</I> MA4680 was expressed using the T7 promoter of the bacterial expression vector pET24ma, over-expressed in <I>Escherichia coli</I> system and characterized. An engineered whole cell system for daidzein hydroxylation was constructed using an exogenous electron transport system from ferredoxin reductase (PdR) and ferredoxin (Pdx). Also, an <I>in vitro</I> reaction study showed the purified CYP105D7 enzyme, using NADH-dependent-reducing equivalents of a redox partner from <I>Pseudomonas putida</I>, hydroxylated daidzein at the 3' position of the B ring to produce 7,3,'4' trihydroxyisoflavone. The hydroxylated position was confirmed by GC-MS analysis. The turnover number of the enzyme was 0.69 &mu;mol 7,3,'4'-trihydroxyisoflavone produced per &mu;mol P450 per min. This enzyme CYP105D7 represents a novel type of 3'-hydroxylase for daidzein hydroxylation. A P450 inhibitor such as coumarin significantly (ca.98%) inhibited the daidzein hydroxylation activity.</P>

발행연도

2013

발행기관

MDPI

라이선스

cc-by

ISSN

1420-3049

18

3

페이지

pp.3028-3040

주제어

enzyme; isoflavone; bioactive compound; hydroxylation; biocatalyst

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논문; 2013-03-06

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