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Synthesis and characterization of PMMA composites activated with starch for immobilization of L-asparaginase

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    • 바이오플라스틱
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    • 바이오정밀화학
      1. 기타
    • 화장품용 기능성소재
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      1. 식품첨가제
논문

Synthesis and characterization of PMMA composites activated with starch for immobilization of L-asparaginase

학술지

Journal of applied polymer science

저자명

Ulu, Ahmet; Koytepe, Suleyman; Ates, Burhan

초록

<P><B>ABSTRACT</B></P><P>Poly (methyl methacrylate) (PMMA)&ndash;starch composites were prepared by emulsion polymerization technique for L&#8208;asparaginase (L&#8208;ASNase) immobilization as highly activated support. The hydroxide groups on the prepared composites offer a very simple, mild and firm combination for enzyme immobilization. The pure PMMA and PMMA&#8208;starch composites were characterized as structural, thermal and morphological. PMMA&#8208;starch composites were found to have better thermal stability and more hydrophilic character than pure PMMA. L&#8208;ASNase was immobilized onto PMMA&#8208;starch composites contained the different ratio of starch (1, 3, 5, and 10 wt %). Immobilized L&#8208;ASNase showed better performance as compared to the native enzyme in terms of thermal stability and pH. <I>K<SUB>m</SUB></I> value of immobilized enzyme decreased approximately eightfold compared with the native enzyme. In addition to, immobilized L&#8208;ASNase was found to retain 60% of activity after 1&#8208;month storage period at 4 &deg;C. Therefore, PMMA&#8208;starch composites can be provided more advantageous in terms of enzymatic affinity, thermal, pH and storage stability as L&#8208;ASNase immobilization matrix. &copy; 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. <B>2016</B>, <I>133</I>, 43421.</P>

발행연도

2016

ISSN

0021-8995

ISSN

1097-4628

133

19

주제어

biodegradable; biomedical applications; biopolymers and renewable polymers; emulsion polymerization

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1 2023-12-11

논문; 2016-02-05

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